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Beilstein J. Org. Chem. 2009, 5, No. 42, doi:10.3762/bjoc.5.42
Graphical Abstract
Figure 1: Benzo[e][2,1]thiazine-4-chloro-3-carbaldehydes 1 and benzo[e][2,1]thiazine-4-chloro-3-carbonitriles ...
Scheme 1: a: NaBH4 (2.5 equiv), MeOH, 2 h, room temp.; b: SOCl2 (4 equiv), benzene, 3 h, 0 °C to room temp.; c...
Scheme 2: a: LiAlH4 (4 equiv), Et2O (THF), 3 h, 0 °C to room temp.; b: HCl saturated in 1,4-dioxane.
Scheme 3: a: AgNO3 (1.5 equiv), NaOH, H2O/CH2Cl2, 3 h, room temp.; b: NaOMe/MeOH, 1 h, reflux; c: PhCH2NH2 (2...